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Area of interest | Chemical Engineering | General & Introductory Chemical Engineering | Available titles | Successful Trouble Shooting for Process Engineers | Table of contents
 

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Contents  
 
Preface XV
1 What is Trouble Shooting? 1
1.1 Characteristics of a Trouble-Shooting Problem 2
1.1.1 Similarities among TS Problems 2
1.1.2 Differences between TS Problems 3
1.2 Characteristics of the Process Used to Solve Trouble-Shooting Problems 3
1.2.1 How the Type of Problem Guides the TS Process or Strategy 3
1.2.2 Five Key Elements Common to the TS Process 4
1.3 Self-Test and Reflections 5
1.4 Overview of the Book 9
1.5 Summary 9
1.6 Cases to Consider 9
2 The Mental Problem-Solving Process used in Trouble Shooting 17
2.1 Problem Solving 19
2.2 Trouble Shooting 23
2.2.1 Considerations when Applying the Strategy to Solve Trouble-Shooting Problems 23
2.2.2 Problem-Solving Processes Used by Skilled Trouble Shooters 24
2.2.3 Data Collection and Analysis: Approaches Used to Test Hypotheses 25
2.3 Overall Summary of Major Skills and a Worksheet 25
2.3.1 Getting Organized: the Use of a Trouble-Shooter´s Worksheet 25
2.3.2 Feedback about your Trouble Shooting 29
2.4 Example Use of the Trouble-Shooter´s Worksheet 35
2.5 Summary 40
2.6 Cases to Consider 40
3 Rules of Thumb for Trouble Shooting 43
3.1 Overall 43
3.1.1 General Rules of Thumb and Typical Causes 43
3.1.2 Corrosion as a Cause 45
3.1.3 Instruments, Valves and Controllers 46
3.1.4 Rules of Thumb for People 47
3.1.5 Trouble-Shooting Teams 48
3.2 Transportation Problems 51
3.2.1 Gas Moving: Pressure Service 52
3.2.2 Gas Moving: Vacuum Service 53
3.2.3 Liquid 54
3.2.4 Solids 56
3.2.5 Steam 58
3.3 Energy Exchange 58
3.3.1 Drives 58
3.3.2 Thermal Energy: Furnaces 60
3.3.3 Thermal Energy: Fluid Heat Exchangers, Condensers and Boilers 61
3.3.4 Thermal Energy: Refrigeration 65
3.3.5 Thermal Energy: Steam Generation 66
3.3.6 High-Temperature Heat-Transfer Fluids 66
3.4 Homogeneous Separation 67
3.4.1 Evaporation 67
3.4.2 Distillation 69
3.4.3 Solution Crystallization 72
3.4.4 Gas Absorption 73
3.4.5 Gas Desorption/Stripping 75
3.4.6 Solvent Extraction, SX 76
3.4.7 Adsorption: Gas 77
3.4.8 Adsorption: Liquid 77
3.4.9 Ion Exchange 77
3.4.10 Membranes: Reverse Osmosis, RO 79
3.4.11 Membranes: Nanofiltration 79
3.4.12 Membranes: Ultrafiltration, UF, and Microfiltration 79
3.5 Heterogeneous Separations 79
3.5.1 Gas-Liquid 80
3.5.2 Gas-Solid 81
3.5.3 Liquid-Liquid 82
3.5.4 Gas-Liquid-Liquid Separators 84
3.5.5 Dryer for GS Separation 85
3.5.6 Screens for Liquid Solid Separation or Dewatering 85
3.5.7 Settlers for LS Separation 86
3.5.8 Hydrocyclones for LS Separation 86
3.5.9 Thickener for LS Separation 86
3.5.10 Sedimentation Centrifuges 87
3.5.11 Filtering Centrifuge 87
3.5.12 Filter for LS Separation 88
3.5.13 Screens for Solid-Solid Separation 88
3.6 Reactor Problems 88
3.6.1 PFTR: Multitube Fixed-Bed Catalyst, Nonadiabatic 89
3.6.2 PFTR: Fixed-Bed Catalyst in Vessel: Adiabatic 91
3.6.3 PFTR: Bubble Reactors, Tray Column Reactors 93
3.6.4 PFTR: Packed Reactors 94
3.6.5 PFTR: Trickle Bed 94
3.6.6 PFTR: Thin Film 96
3.6.7 STR: Batch (Backmix) 96
3.6.8 STR: Semibatch 98
3.6.9 CSTR: Mechanical Mixer (Backmix) 99
3.6.10 STR: Fluidized Bed (Backmix) 101
3.6.11 Mix of CSTR, PFTR with Recycle 106
3.6.12 Reactive Extrusion 106
3.7 Mixing Problems 107
3.7.1 Mechanical Agitation of Liquid 107
3.7.2 Mechanical Mixing of Liquid-Solid 108
3.7.3 Solids Blending 108
3.8 Size-Decrease Problems 109
3.8.1 Gas Breakup in Liquid: Bubble Columns 109
3.8.2 Gas Breakup in Liquid: Packed Columns 109
3.8.3 Gas Breakup in Liquid: Agitated Tanks 110
3.9 Size Enlargement 110
3.9.1 Size Enlargement: Liquid-Gas: Demisters 110
3.9.2 Size Enlargement: Liquid-Liquid: Coalescers 110
3.9.3 Size Enlargement: Solid in Liquid: Coagulation/Flocculation 111
3.9.4 Size Enlargement: Solids: Tabletting 111
3.9.5 Size Enlargement: Solids: Pelleting 111
3.9.6 Solids: Modify Size and Shape: Injection Molding and Extruders 112
3.9.7 Coating 126
3.10 Vessels, Bins, Hoppers and Storage Tanks 126
3.11 ‘‘Systems’‘ Thinking 127
3.12 Health, Fire and Stability 130
3.12.1 Individual Species 130
3.12.2 Combinations 131
4 Trouble Shooting in Action: Examples 133
4.1 Case #3: The Case of the Cycling Column 133
4.2 Case #4: Platformer Fires 138
4.3 Case #5: The Sulfuric Acid Pump 141
4.4 Case #6: The Case of the Utility Dryer 144
4.5 Case #7: The Case of the Reluctant Crystallizer 157
4.6 Reflections about these Examples 162
5 Polishing Your Skills: Problem-Solving Process 165
5.1 Developing Awareness of the Problem-Solving Process 165
5.1.1 Some Target Skills 166
5.1.2 The TAPPS Roles: Talker and Listener 166
5.1.3 Activity 5.1: (35 minutes) 168
5.1.4 Feedback, Self-Assessment 172
5.2 Strategies 173
5.2.1 Some Target Skills 174
5.2.2 The Extended TAPPS Roles: Talker+ and Listener+ 175
5.2.3 Activity 5.2: (time 35 minutes) 176
5.2.4 Feedback, Self-assessment 179
5.3 Exploring the ‘‘Context’‘: what is the Real Problem? 180
5.3.1 Example 180
5.3.2 Activity 5-3 181
5.4 Creativity 183
5.4.1 Some Target Skills 183
5.4.2 Example: Case #10: To dry or not to dry! (based on Krishnaswamy and Parker, 1984) 186
5.4.3 Activity 5-4 190
5.4.4 Feedback, Self-Assessment 191
5.5 Self-Assessment 191
5.5.1 Some Target Skills 192
5.5.2 Activity for Growth in Self-Assessment 192
5.5.3 Feedback About Assessment 193
5.6 Summary and Self-Rating 194
6 Polishing Your Skills: Gathering Data and the Critical-Thinking Process 195
6.1 Thinking Skills: How to Select Valid Diagnostic Actions 196
6.1.1 How to Select a Diagnostic Action 196
6.1.2 Select from among a Range of Diagnostic Actions 196
6.1.3 More on Gathering and Interpreting Data 200
6.1.4 Summary 209
6.2 Thinking Skill: Consistency: Definitions, Cause-Effect and Fundamentals 209
6.2.1 Consistent Use of Definitions 210
6.2.2 Consistent with How Equipment Works: Cause Effects: Root Cause-Symptoms 212
6.2.3 Consistent with Fundamental Rules of Mathematics and English 217
6.2.4 Consistent with Fundamental Principles Of Science: Conservation of Mass, Energy, High to Low Pressure, Properties of Materials 218
6.2.5 Consistent with Experience 218
6.2.6 Summary 219
6.3 Thinking Skills: Classification 219
6.3.1 Classify the Starting Information 219
6.3.2 Classifying Ideas from Brainstorming 220
6.4 Thinking Skills: Recognizing Patterns 221
6.4.1 Patterns in the Symptoms 221
6.4.2 Patterns in the Evidence 223
6.5 Thinking Skill: Reasoning 223
6.5.1 Step 1: Classify the Information 224
6.5.2 Step 2: Write the Conclusion 225
6.5.3 Step 3: Identify the Context 225
6.5.4 Step 4: Clarify the Meaning of the Terminology 226
6.5.5 Step 5: Consider the Evidence 227
6.5.5a Identify the Evidence 227
6.5.5b Check for Consistency 227
6.5.5c Which Evidence is Pertinent? 228
6.5.5d Diagram the Argument 229
6.5.6 Step 6: Formulate the Assumptions 230
6.5.7 Step 7: Assess the Quality of the Reasoning 230
6.5.8 Step 8: Assess the Strengths of the Counterarguments 232
6.5.9 Step 9: Evaluate the Consequences and Implications 232
6.5.10 Activity 6-14 232
6.6 Feedback and Self-Assessment 233
6.7 Summary 233
6.8 Exercises 234
7 Polishing Your Skills: Interpersonal Skills and Factors Affecting Personal Performance 237
7.1 Interpersonal Skills 237
7.1.1 Communication 237
7.1.2 Listening 238
7.1.3 Fundamentals of Interaction 239
7.1.4 Trust 240
7.1.5 Building on Another´s Personal Uniqueness 243
7.2 Factors that Affect Personal Performance 244
7.2.1 Pride and Unwillingness to Admit Error 244
7.2.2 Stress: Low and High Stress Errors 245
7.2.3 Alienation and Lack of Motivation 249
7.2.4 ‘‘I Know Best!’‘ Attitude 249
7.2.5 Tendency to Interpret 249
7.3 The Environment 253
7.4 Summary 253
7.5 Exercises and Activities 253
8 Prescription for Improvement: Put it all Together 259
8.1 Approaches to Polish Your Skill 259
8.1.1 Triad Activity 259
8.1.2 Individual Activity 262
8.2 Cases to Help you Polish Your Skill 263
8.2.1 Guidelines for Selecting a Case 263
8.2.2 The Cases and Understanding the Choice of Diagnostic Actions for each Case 263
8.3 Summary 396
9 What Next? 397
9.1 Summary of Highlights 397
9.2 Reflection and Self-Assessment are Vital for the Development of Confidence 401
9.3 Going Beyond this Book: Setting Goals for Improvement 402
9.3.1 Prepare Yourself for Success 402
9.3.2 Use Reflection and Self-Assessment Effectively 403
9.4 Going Beyond this Book: Updating your Rules of Thumb and Symptom Cause Data for Process Equipment 403
9.5 Beyond this Book: Sources of Other Cases 403
Literature References 405
Index I 1
CD Contents
Appendix A
Feedback about Experience with Process Equipment
411
Appendix B
Improving ‘‘Systems Thinking’‘
415
Appendix C
Feedback on the Cases in Chapters 1, 2 and 7
423
Appendix D
Coded Answers for the Questions Posed to Solve the Cases
435
Appendix E
Debrief for the Trouble-Shooting Cases
537
Appendix F
Other Tasks for the Skill-Development Activities in Chapter 5
565
Appendix G
Selected Responses to the Activities in Chapters 6 and 7
569
Appendix H
Data about ‘‘Causes’’ for Selected Process Equipment
573
Appendix I
Feedback about Symptoms for Selected Causes
579
Appendix J
Guide for Students: How You Can Get the Most from this Book
581
J-1 Getting Started: Get the Big Picture 581
J-2 Try a Trouble-Shooting Case where the Problem is Reasonably Well Defined 582
J-3 See How Others Handle a Case 591
J-4 Pause, Reflect on the Pretest, and Invest Time Polishing Specific Skills 591
J-5 Work your First Cases Starting with Case #19 591
J-6 Trouble Shooting on the Job 591
J-7 Summary 592

 





 

        

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