Mayo, Dana W. / Pike, Ronald M. / Forbes, David C. Microscale Organic Laboratory with Multistep and Multiscale Syntheses
5. Edition - February 2010 189.- Euro 2010. 704 Pages, Hardcover ISBN-10: 0-471-21502-3 ISBN-13: 978-0-471-21502-8 - John Wiley & Sons
Short description The fifth edition provides complete coverage of organic laboratory experiments and techniques for organic chemists. The book offers the flexibility of creating one's own scaling sequence without being tied to prescribed set of quantities. It presents a strong emphasis on modern laboratory instrumentation along with a sharp focus on safety in the lab. The experimental procedure section is divided into four subsections, allowing them to effortlessly organize their laboratory time. It now covers green chemistry to offer the latest information in the field. A rich collection of end of chapter exercises and new pre- and post-lab questions also nurture success among organic chemists.
From the contents * Chapter One - Introduction * Chapter Two - Safety * Chapter Three - Introduction to Microscale Organic Laboratory Equipment and Techniques * Chapter Four - Determination of Physical Properties * Chapter Five - Microscale Laboratory Techniques * Chapter Six - Microscale Organic Laboratory Experiments * Chapter Seven - Sequential Syntheses: The Transition from Macro to Micro * Chapter Eight - Spectroscopic Identification of Organic Compounds * Chapter Nine - Qualitative Identification of Organic Compounds * Chapter Ten (Online) - Advanced Microscale Organic Laboratory Experiments
