Two-Dimensional NMR Methods for Establishing Molecular Connectivity
A Chemist's Guide to Experiment Selection, Performance, and Interpretation
Methods in Stereochemical Analysis (Series Nr. 12)
1. Edition October 1988
XX, 508 Pages, Hardcover
245 Pictures
48 tables
Monograph
This guide to two-dimensional NMR spectroscopy helps the novice who want e the technique, but needs a path through the bewildering array of metho acronyms and the mathematical rigor found in most books.
The authors provide a clear explanation of experiment performance, param lection, data processing and presentation as well as a description of wh rmation is provided by each experiment and how it is extracted and inter They group presentations of two-dimensional NMR experiments according t zation, e.g. COSY, LRCOSY, ZQCOSY, DQCOSY ... for establishing proton-pr nnectivities.
The book also presents spectra of the same model compound using various ues to enable the reader to make direct comparisons and facilitate his e nt selection. Examples of the concerted utilization of various two-dimen NMR experiments to solve complex structural problems are also given.
Heteronuclear Chemical shift Correlation.
Relayed Coherence Transfer and Related 2D-NMR Experiments.
13_C-13_C Double Coherence 2D-NMR. The Inadequate Experiments.
Applications Problems.
Solutions to Problems.
Index.